• Multi Detector Characterisation of Polymer Nanogels
    Set-up for static and dynamic light scattering measurement.
  • Testa Analytical triple detection GPC/SEC system.
  • Researchers from the Division of Applied Radiation Chemistry.

Chromatography

Multi Detector Characterisation of Polymer Nanogels

Apr 09 2021

Testa Analytical Solutions eK reports how researchers at Lodz University of Technology have combined the advanced analytical capabilities of its GPC/SEC triple detection system with a BI-200SM light scattering goniometer to derive in-depth information about an exciting new generation of polymer nanogels.

Dr Slawomir Kadlubowski the Associate Professor of the Division of Applied Radiation Chemistry said: "To advance our characterisation capabilities we have invested in a number of methods to analyse the physico-chemical properties of the polymer nanogels that we synthesise. This includes static and dynamic light scattering using a research grade goniometer and Gel Permeation Chromatography (GPC) with triple detection (MALLS, DRI, Viscometer). Combining these methods, we are able to determine changes in molecular weight and size (or their distribution) during synthesis and to have a full view on interactions between chain segments or macromolecules. This leads not only for understanding of mechanism of intramolecular crosslinking, which is a basic reaction for nanogel synthesis, but also to obtain product with the properties required by a specific practical application such as a drug delivery system. We chose to purchase the triple detection GPC system and the light scattering goniometer from Testa Analytical not only because of the excellent performance and versatility of their systems but also because of the informed technical support they supply allowing us to get the best out of these instruments."


Testa Analytical Solutions has developed a range of highly sensitive detectors (Viscometry, DRI, UV, MALLS, Flowmeter) that can be used as part of a triple detector GPC/SEC system to determine the size and conformation of all types of synthetic polymers, biopolymers, proteins, and peptides. The company is also able to offer polymer researchers - the Bl-200SM light scattering goniometer - a precision research grade instrument designed for precise and accurate measurements. Based on a special turntable with precision ball bearings and stepping motor, the Bl-200SM's modular, automated design and quality construction guarantee precise measurements due to the wobble-free movement of the detector. The BI-200SM can measure light scattering over a wide angular range (8° to 155° with 25 mm cells) and offers fine adjustment of measurement angles to 0.01° directly using a large, fine-control knob or PC-driven motor control.

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